QUICK TESTS FOR SOME ADULTERANTS IN FOOD


 

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SPICES AND CONDIMENTS


Name of Food Article Adulterant

Simple Method for detection of Common Adulterants

Remarks

i. Whole spices Dirt, dust, straw, insect, damaged seeds, other seeds, rodent hair and excreta. These can be examined visually.  
a.Black pepper Papaya seeds Papaya seeds can be separated out from pepper as they are shrunken, oval in shape and greenish brown or brownish black in colour.  
  Light black pepper Float the sample of black pepper in alcohol (rectified spirit). The mature black pepper beries sink while the papaya seeds and light black pepper float.  
  Coated with mineral oil Black pepper coated with mineral oil gives Kerosene like smell.  
b.Cloves Volatile oil extracted (exhausted cloves) Exhausted cloves can be identified by its small size and shrunken appearance. The characteristic pungent tests of genuine cloves is less pronounced in exhausted cloves.  
c. Mustard seed Argemone seed Mustard seeds have a smooth surface. the argemone seed have grainy and rough surface and are black and hence can be separated out by close examination. When Mustard seed is pressed inside it is yellow while for argemone seed it is white. Use magnifying glass for identification.
ii.Powdered spices Added starch


Common Salt
Add a few drops of tincture of lodine or lodine solution. Indication of blue colour shows the presence of starch.

Taste for addition of common salt.
Iodine test for added starch is not applicable for turmeric powder.
a. Turmeric powder Coloured saw dust





Chalk powder or yellow soap stone powder
Take a tea spoon full of turmeric powder in a test tube. Ad a few drops of concentrated Hydrochloric acid. Instant appearance of pink colour which disappears on dilution with water shows the presence of turmeric. If the colour persists, metanil yellow (an artificial colour) a non-permitted coal tar colour is present.

Take a small quantity of turmeric powder in a test tube containing small quantity of water. Add a few drops of concentrated Hydrochloric acid, effervescence (give off bubbles) will indicate the presence of chalk or yellow soap stone powder.
This test is only for Metanil yellow.
b. Chillies powder Brick Powder, salt powder or talc powder.




Water soluble coal tar colour
Take a tea spoon full of chillies powder in a glass of water. Coloured water extract will show the presence of articficial colour. Any grittingess that may be felt on rubbing the sediment at the bottom of glass confirms the presence of brick powder/sand, soapy and smooth touch of the white residue at the bottom indicates the presence of soap stone.

Water soluble artificial colour can be detected by sprinkling s small quantity of chillies or turmeric powder on the surface of water contained in a glass tumbler. The water soluble colour will immediately start descending in colour streaks.
This test is only for earthy material.
  Oil solube coat tar colour Take 2 gms of the samples in a test tube, add few ml of solvent ether and shake, Decant ether layer into a test tube containing 2ml of dilute Hydrochloric acid (1 ml HCl plus 1ml of water). Shake it, the lower acid layer wil be coloured distinct pink to red indicating presence of oil soluble colour. See also Appendix-I.
iii. Hing Soap stone or other earthy matter Shake little portion of the sample with water and allow to settle. Soap stone or other earthy matter will settle down at the bottom. In compounded hing due to presence of starch, a slight turbid solution, may be produced. However, this will settle down after keeping.
iv. Saffron Dried tendrils of maize cob Genuine saffron will not break easily like artificial. Artificial